Characterization and 2D structural model of corn straw and poplar leaf biochars.
Identifieur interne : 001008 ( Main/Exploration ); précédent : 001007; suivant : 001009Characterization and 2D structural model of corn straw and poplar leaf biochars.
Auteurs : Nan Zhao [République populaire de Chine] ; Yizhong Lv [République populaire de Chine, Canada] ; Xixiang Yang [Japon] ; Feng Huang [République populaire de Chine] ; Jianwen Yang [Canada]Source :
- Environmental science and pollution research international [ 1614-7499 ] ; 2018.
Descripteurs français
- KwdFr :
- MESH :
- composition chimique : Charbon de bois, Feuilles de plante, Tiges de plante.
- Carbone, Populus, Spectroscopie infrarouge à transformée de Fourier, Température, Température élevée, Zea mays.
English descriptors
- KwdEn :
- MESH :
- chemical , chemistry : Charcoal.
- chemical : Carbon.
- chemistry : Plant Leaves, Plant Stems.
- Hot Temperature, Populus, Spectroscopy, Fourier Transform Infrared, Temperature, Zea mays.
Abstract
The integrated experimental methods were used to analyze the physicochemical properties and structural characteristics and to build the 2D structural model of two kinds of biochars. Corn straw and poplar leaf biochars were gained by pyrolysing the raw materials slowly in a furnace at 300, 500, and 700 °C under oxygen-deficient conditions. Scanning electron microscope was applied to observe the surface morphology of the biochars. High temperatures destroyed the pore structures of the biochars, forming a particle mixture of varying sizes. The ash content, yield, pH, and surface area were also observed to describe the biochars' properties. The yield decreases as the pyrolysis temperature increases. The biochars are neutral to alkaline. The biggest surface area is 251.11 m2/g for 700 °C corn straw biochar. Elemental analysis, infrared microspectroscopy, solid-state C-13 NMR spectroscopy, and pyrolysis gas chromatography-mass spectrometry (Py-GC-MS) were also used to study the structural characteristics and build the 2D structural models of biochars. The C content in the corn straw and poplar leaf biochars increases with the increase of the pyrolysis temperature. A higher pyrolysis temperature makes the aryl carbon increase, and C=O, OH, and aliphatic hydrocarbon content decrease in the IR spectra. Solid-state C-13 NMR spectra show that a higher pyrolysis temperature makes the alkyl carbon and alkoxy carbon decrease and the aryl carbon increase. The results of IR microspectra and solid-state C-13 NMR spectra reveal that some noticeable differences exist in these two kinds of biochars and in the same type of biochar but under different pyrolysis temperatures. The conceptual elemental compositions of 500 °C corn straw and poplar leaf biochars are C61H33NO13 and C59H41N3O12, respectively. Significant differences exist in the SEM images, physicochemical properties, and structural characteristics of corn straw and poplar leaf biochars.
DOI: 10.1007/s11356-017-0959-1
PubMed: 29270898
Affiliations:
- Canada, Japon, République populaire de Chine
- Kyūshū, Préfecture de Fukuoka
- Fukuoka
- Université de Kyūshū
Links toward previous steps (curation, corpus...)
Le document en format XML
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wicri:level="1"><nlm:affiliation>School of Environmental Science and Engineering, Guangdong Provincial Key Lab of Environmental Pollution Control and Remediation Technology, Sun Yat-sen University, Guangzhou, 510275, People's Republic of China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>School of Environmental Science and Engineering, Guangdong Provincial Key Lab of Environmental Pollution Control and Remediation Technology, Sun Yat-sen University, Guangzhou, 510275</wicri:regionArea><wicri:noRegion>510275</wicri:noRegion></affiliation><affiliation wicri:level="1"><nlm:affiliation>College of Resources and Environmental Sciences, China Agricultural University, Beijing, 100193, People's Republic of China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>College of Resources and Environmental Sciences, China Agricultural University, Beijing, 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(MeSH)</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Charcoal</term></keywords><keywords scheme="MESH" type="chemical" xml:lang="en"><term>Carbon</term></keywords><keywords scheme="MESH" qualifier="chemistry" xml:lang="en"><term>Plant Leaves</term><term>Plant Stems</term></keywords><keywords scheme="MESH" qualifier="composition chimique" xml:lang="fr"><term>Charbon de bois</term><term>Feuilles de plante</term><term>Tiges de plante</term></keywords><keywords scheme="MESH" xml:lang="en"><term>Hot Temperature</term><term>Populus</term><term>Spectroscopy, Fourier Transform Infrared</term><term>Temperature</term><term>Zea mays</term></keywords><keywords scheme="MESH" xml:lang="fr"><term>Carbone</term><term>Populus</term><term>Spectroscopie infrarouge à transformée de Fourier</term><term>Température</term><term>Température élevée</term><term>Zea mays</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">The integrated experimental methods were used to analyze the physicochemical properties and structural characteristics and to build the 2D structural model of two kinds of biochars. Corn straw and poplar leaf biochars were gained by pyrolysing the raw materials slowly in a furnace at 300, 500, and 700 °C under oxygen-deficient conditions. Scanning electron microscope was applied to observe the surface morphology of the biochars. High temperatures destroyed the pore structures of the biochars, forming a particle mixture of varying sizes. The ash content, yield, pH, and surface area were also observed to describe the biochars' properties. The yield decreases as the pyrolysis temperature increases. The biochars are neutral to alkaline. The biggest surface area is 251.11 m<sup>2</sup>/g for 700 °C corn straw biochar. Elemental analysis, infrared microspectroscopy, solid-state C-13 NMR spectroscopy, and pyrolysis gas chromatography-mass spectrometry (Py-GC-MS) were also used to study the structural characteristics and build the 2D structural models of biochars. The C content in the corn straw and poplar leaf biochars increases with the increase of the pyrolysis temperature. A higher pyrolysis temperature makes the aryl carbon increase, and C=O, OH, and aliphatic hydrocarbon content decrease in the IR spectra. Solid-state C-13 NMR spectra show that a higher pyrolysis temperature makes the alkyl carbon and alkoxy carbon decrease and the aryl carbon increase. The results of IR microspectra and solid-state C-13 NMR spectra reveal that some noticeable differences exist in these two kinds of biochars and in the same type of biochar but under different pyrolysis temperatures. The conceptual elemental compositions of 500 °C corn straw and poplar leaf biochars are C<sub>61</sub>H<sub>33</sub>NO<sub>13</sub> and C<sub>59</sub>H<sub>41</sub>N<sub>3</sub>O<sub>12</sub>, respectively. Significant differences exist in the SEM images, physicochemical properties, and structural characteristics of corn straw and poplar leaf biochars.</div></front></TEI><pubmed><MedlineCitation Status="MEDLINE" IndexingMethod="Curated" Owner="NLM"><PMID Version="1">29270898</PMID><DateCompleted><Year>2019</Year><Month>01</Month><Day>01</Day></DateCompleted><DateRevised><Year>2019</Year><Month>01</Month><Day>01</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1614-7499</ISSN><JournalIssue CitedMedium="Internet"><Volume>25</Volume><Issue>26</Issue><PubDate><Year>2018</Year><Month>Sep</Month></PubDate></JournalIssue><Title>Environmental science and pollution research international</Title><ISOAbbreviation>Environ Sci Pollut Res Int</ISOAbbreviation></Journal><ArticleTitle>Characterization and 2D structural model of corn straw and poplar leaf biochars.</ArticleTitle><Pagination><MedlinePgn>25789-25798</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1007/s11356-017-0959-1</ELocationID><Abstract><AbstractText>The integrated experimental methods were used to analyze the physicochemical properties and structural characteristics and to build the 2D structural model of two kinds of biochars. Corn straw and poplar leaf biochars were gained by pyrolysing the raw materials slowly in a furnace at 300, 500, and 700 °C under oxygen-deficient conditions. Scanning electron microscope was applied to observe the surface morphology of the biochars. High temperatures destroyed the pore structures of the biochars, forming a particle mixture of varying sizes. The ash content, yield, pH, and surface area were also observed to describe the biochars' properties. The yield decreases as the pyrolysis temperature increases. The biochars are neutral to alkaline. The biggest surface area is 251.11 m<sup>2</sup>/g for 700 °C corn straw biochar. Elemental analysis, infrared microspectroscopy, solid-state C-13 NMR spectroscopy, and pyrolysis gas chromatography-mass spectrometry (Py-GC-MS) were also used to study the structural characteristics and build the 2D structural models of biochars. The C content in the corn straw and poplar leaf biochars increases with the increase of the pyrolysis temperature. A higher pyrolysis temperature makes the aryl carbon increase, and C=O, OH, and aliphatic hydrocarbon content decrease in the IR spectra. Solid-state C-13 NMR spectra show that a higher pyrolysis temperature makes the alkyl carbon and alkoxy carbon decrease and the aryl carbon increase. The results of IR microspectra and solid-state C-13 NMR spectra reveal that some noticeable differences exist in these two kinds of biochars and in the same type of biochar but under different pyrolysis temperatures. The conceptual elemental compositions of 500 °C corn straw and poplar leaf biochars are C<sub>61</sub>H<sub>33</sub>NO<sub>13</sub> and C<sub>59</sub>H<sub>41</sub>N<sub>3</sub>O<sub>12</sub>, respectively. Significant differences exist in the SEM images, physicochemical properties, and structural characteristics of corn straw and poplar leaf biochars.</AbstractText></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Zhao</LastName><ForeName>Nan</ForeName><Initials>N</Initials><AffiliationInfo><Affiliation>School of Environmental Science and Engineering, Guangdong Provincial Key Lab of Environmental Pollution Control and Remediation Technology, Sun Yat-sen University, Guangzhou, 510275, People's Republic of China.</Affiliation></AffiliationInfo><AffiliationInfo><Affiliation>College of Resources and Environmental Sciences, China Agricultural University, Beijing, 100193, People's Republic of China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Lv</LastName><ForeName>YiZhong</ForeName><Initials>Y</Initials><AffiliationInfo><Affiliation>College of Resources and Environmental Sciences, China Agricultural University, Beijing, 100193, People's Republic of China. lyz@cau.edu.cn.</Affiliation></AffiliationInfo><AffiliationInfo><Affiliation>Department of Earth and Environmental Sciences, University of Windsor, Windsor, ON, N9B 3P4, Canada. lyz@cau.edu.cn.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Yang</LastName><ForeName>XiXiang</ForeName><Initials>X</Initials><AffiliationInfo><Affiliation>Department of Applied Chemistry, Graduate School of Engineering, Kyushu University, 744 Motooka, Nishi-ku, Fukuoka, 819-0395, Japan.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Huang</LastName><ForeName>Feng</ForeName><Initials>F</Initials><AffiliationInfo><Affiliation>College of Resources and Environmental Sciences, China Agricultural University, Beijing, 100193, People's Republic of China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Yang</LastName><ForeName>JianWen</ForeName><Initials>J</Initials><AffiliationInfo><Affiliation>Department of Earth and Environmental Sciences, University of Windsor, Windsor, ON, N9B 3P4, Canada.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><GrantList CompleteYN="Y"><Grant><GrantID>41271331</GrantID><Agency>National Natural Science Foundation of China</Agency><Country></Country></Grant><Grant><GrantID>2016M591267</GrantID><Agency>China Postdoctoral Science Foundation</Agency><Country></Country></Grant></GrantList><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2017</Year><Month>12</Month><Day>22</Day></ArticleDate></Article><MedlineJournalInfo><Country>Germany</Country><MedlineTA>Environ Sci Pollut Res Int</MedlineTA><NlmUniqueID>9441769</NlmUniqueID><ISSNLinking>0944-1344</ISSNLinking></MedlineJournalInfo><ChemicalList><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="C540010">biochar</NameOfSubstance></Chemical><Chemical><RegistryNumber>16291-96-6</RegistryNumber><NameOfSubstance UI="D002606">Charcoal</NameOfSubstance></Chemical><Chemical><RegistryNumber>7440-44-0</RegistryNumber><NameOfSubstance UI="D002244">Carbon</NameOfSubstance></Chemical></ChemicalList><CitationSubset>IM</CitationSubset><MeshHeadingList><MeshHeading><DescriptorName UI="D002244" MajorTopicYN="N">Carbon</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D002606" MajorTopicYN="N">Charcoal</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D006358" MajorTopicYN="N">Hot Temperature</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D018515" MajorTopicYN="N">Plant Leaves</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D018547" MajorTopicYN="N">Plant Stems</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D032107" MajorTopicYN="Y">Populus</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D017550" MajorTopicYN="N">Spectroscopy, Fourier Transform Infrared</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D013696" MajorTopicYN="N">Temperature</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D003313" MajorTopicYN="Y">Zea mays</DescriptorName></MeshHeading></MeshHeadingList><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">2D structural modelings</Keyword><Keyword MajorTopicYN="N">Biochar characteristics</Keyword><Keyword MajorTopicYN="N">Corn straw</Keyword><Keyword MajorTopicYN="N">Poplar leaf</Keyword><Keyword MajorTopicYN="N">Pyrolysis temperature</Keyword></KeywordList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2016</Year><Month>12</Month><Day>27</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>2017</Year><Month>12</Month><Day>06</Day></PubMedPubDate><PubMedPubDate 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sort="Zhao, Nan" uniqKey="Zhao N" first="Nan" last="Zhao">Nan Zhao</name></noRegion><name sortKey="Huang, Feng" sort="Huang, Feng" uniqKey="Huang F" first="Feng" last="Huang">Feng Huang</name><name sortKey="Lv, Yizhong" sort="Lv, Yizhong" uniqKey="Lv Y" first="Yizhong" last="Lv">Yizhong Lv</name><name sortKey="Zhao, Nan" sort="Zhao, Nan" uniqKey="Zhao N" first="Nan" last="Zhao">Nan Zhao</name></country><country name="Canada"><noRegion><name sortKey="Lv, Yizhong" sort="Lv, Yizhong" uniqKey="Lv Y" first="Yizhong" last="Lv">Yizhong Lv</name></noRegion><name sortKey="Yang, Jianwen" sort="Yang, Jianwen" uniqKey="Yang J" first="Jianwen" last="Yang">Jianwen Yang</name></country><country name="Japon"><region name="Kyūshū"><name sortKey="Yang, Xixiang" sort="Yang, Xixiang" uniqKey="Yang X" first="Xixiang" last="Yang">Xixiang Yang</name></region></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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